What is the function of ionization chamber in mass spectrometer?

Structure of the mass spectrometer The ionization chamber is a region where atoms of unknown material are excited to cause them to lose electrons. Sometimes, the energy needed to excite atoms is obtained simply by heating the sample. The ionization chambers consist of a pair of charged electrodes that collect the ions formed within their respective electric fields. Ionization chambers can measure the dose or dose rate because they provide an indirect representation of the energy deposited in the chamber.

The vaporized sample passes to the ionization chamber. The electrically heated metal coil emits electrons that are attracted to the electron trap, which is a positively charged plate. All types of these devices have a filter in the opening of the chamber to prevent the passage of particulate radioactive materials, such as radon decay products, into the chamber. When the atoms or gas molecules between the electrodes are ionized by the incident ionizing radiation, ion pairs are created and the resulting positive ions are created and the dissociated electrons move to the electrodes of the opposite polarity under the influence of the electric field.

The ionization chamber is the only gas-filled detector that allows direct determination of the absorbed dose. A positively charged electret is used together with an ionization chamber made of an electrically conductive plastic. Operation as an ionization chamber involves the use of an applied voltage that is large enough to collect all of the ion pairs (positive ion and electron removed) produced in the gas by a radioactive source, but not large enough to cause any amplification of the gas. The ICP has the ability to ionize almost all elements, including those with the highest ionization potentials.

It is important that the ions produced in the ionization chamber pass freely through the machine without colliding with air molecules. Positively charged ionization chamber repels positively charged ions, which accelerate to three negatively charged slits with progressively decreasing voltage. Sometimes two mass spectrometers are paired, so that a gentle ionization method can be followed by a more vigorous ionization of the individual fragments. Multi-cavity ionization chambers can measure the intensity of the radiation beam in several different regions, providing information on the symmetry and flatness of the beam.

The sample is vaporized before passing it to an ionization chamber where it is bombarded by a current of electrons emitted by an electrically heated metal coil. A more recent application of primitive total ionization chambers (such as the electroscopes used, for example, by Rutherford in the early 20th century), is based on the use of an electret, which maintains a charge for an extended period and is discharged by exposure to radiation. A gas ionization chamber measures charge from the number of ion pairs created within a gas caused by incident radiation. In other words, all the energy of the primary electrons produced in the sensitive volume of the chamber must dissipate in the chamber.

Ionization chambers are widely used in the nuclear industry, as they provide an output that is proportional to the radiation dose. They find wide use in situations where a constant high dose rate is measured, as they have a longer useful life than standard Geiger-Müller tubes, which suffer from gas, decompose and are generally limited to a life of approximately 10-11 counting events. In the IC, a gas (commonly methane, ammonia, or isobutane) is introduced into an EI ionization chamber at a concentration higher than that of the analyte. .

Jada Urquiza
Jada Urquiza

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